化工社化工社 化学情報印刷レポート · 研究参考用
Ethamivan → Methyl-phenyl-carbamic Acid 4-diethylcarbamoyl-2-methoxy-phenyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethamivan | HCID 9363 | — |
| 反応物 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 生成物 | Methyl-phenyl-carbamic Acid 4-diethylcarbamoyl-2-methoxy-phenyl Ester | HCID 69519834 | — |
反応手順
The title product was prepared from N,N-diethyl-4-hydroxy-3-methoxy-benzamide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (58%, colorless oil). HPLC-MS: m/z=357.1 (M+1); Rt: 3.64 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07279470B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-b926100beef34922845287d820e3c1cd |
| 出典メモ | uspto-grants-2007_10 |