化工社化工社 化学情報印刷レポート · 研究参考用
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-morpholin-4-yl-phenyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 反応物 | 4-Morpholinophenol | HCID 80510 | — |
| 生成物 | Methyl-phenyl-carbamic Acid 4-morpholin-4-yl-phenyl Ester | HCID 10171887 | — |
反応手順
The title product was prepared from and 4-morpholin-4-yl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was extracted with dichloromethane from citric acid (5%). The combined organic phases were evaporated and the product crystallized from ethanol (22%, crystals). HPLC-MS: m/z=313.2 (M+1); Rt: 3.75 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07279470B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-f6fd6e4b0ece44aca54192f6f8bc038b |
| 出典メモ | uspto-grants-2007_10 |