化工社化工社 化学情報印刷レポート · 研究参考用
4'-Hydroxybutyranilide → Methyl-phenyl-carbamic Acid 4-butyrylamino-phenyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4'-Hydroxybutyranilide | HCID 66874 | — |
| 反応物 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 生成物 | Methyl-phenyl-carbamic Acid 4-butyrylamino-phenyl Ester | HCID 69519645 | — |
反応手順
The title product was prepared from 4′-hydroxybutyranilide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (60%, white solid). HPLC-MS: m/z=313.2 (M+1); Rt: 3.58 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07279470B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-df532a5ea6d146e7a08d6bb5c852fb0c |
| 出典メモ | uspto-grants-2007_10 |