化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Bromide → 4-Cyclohexylmethyl-piperazine-1-carboxylic Acid 4-(3-chloro-5-trifluoromethyl-pyridin-2-yloxy)-phenyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Bromide | HCID 253877 | — |
| 反応物 | 1-(Cyclohexylmethyl)piperazine | HCID 2735885 | — |
| 反応物 | 4-(3-Chloro-5-trifluoromethylpyridin-2-yloxy)-phenyl chloroformate | HCID 22047691 | — |
| 生成物 | 4-Cyclohexylmethyl-piperazine-1-carboxylic Acid 4-(3-chloro-5-trifluoromethyl-pyridin-2-yloxy)-phenyl Ester | HCID 69518167 | — |
反応手順
The hydrochloride of the title compound was prepared from 4-(3-chloro-5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 1-cyclohexylmethyl-piperazine, yield 76%. White crystals, m.p. 265-266° C.; IR (KBr): ν 1732 (C═O) cm−1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07279470B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-5e2a401ef55446f6994f8f54f83438da |
| 出典メモ | uspto-grants-2007_10 |