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1-((4-Methoxyphenyl)methyl)piperazine → 4-(4-Methoxy-benzyl)-piperazine-1-carboxylic Acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-((4-Methoxyphenyl)methyl)piperazine | HCID 231905 | — |
| 反応物 | 4-(4,4-Dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl chloroformate | HCID 22047895 | — |
| 生成物 | 4-(4-Methoxy-benzyl)-piperazine-1-carboxylic Acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester | HCID 57455837 | — |
反応手順
The title compound was prepared from 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl chloroformate and 1-(4-methoxybenzyl)-piperazine, preparative HPLC (Method C) (54%, white crystals). HPLC-MS m/z=466.3 (M+1), Rt: 2.26 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07279470B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-e0029471ee6d40fc9b6386dc110dda75 |
| 出典メモ | uspto-grants-2007_10 |