化工社化工社 化学情報印刷レポート · 研究参考用
Benzoyl chloride → 4-Methoxybenzophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl chloride | HCID 7412 | — |
| 反応物 | Anisole | HCID 7519 | — |
| 反応物 | Boron carbide | HCID 123279 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 4-Methoxybenzophenone | HCID 69146 | 48.2% |
反応手順
A mixture of 5.4 gm (0.05 moles) of anisole and 7.0 gm (0.05) moles of benzoyl chloride and 0.5 gm of boron carbide was placed in 50 ml of benzene. This mixture was allowed to react as described in Example 3. A yield of 48.2% of p-methoxy benzophenone was obtained, and 0.5 gm of the boron carbide catalysts was recovered.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07279604B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-1185fc3e6a64469d9b8dbfeb70c90873 |
| 出典メモ | uspto-grants-2007_10 |