化工社化工社 化学情報印刷レポート · 研究参考用
4,4'-Dibromostilbene → 4,4'-bis[N-(dibenzofuran-2-yl)-N-phenylamino]stilbene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4,4'-Dibromostilbene | HCID 53395981 | — |
| 反応物 | N-phenyl-2-Dibenzofuranamine | HCID 67204676 | — |
| 溶媒 | Ethyl acetate hexane | HCID 21226206 | — |
| 生成物 | 4,4'-bis[N-(dibenzofuran-2-yl)-N-phenylamino]stilbene | HCID 68109724 | — |
反応手順
The Rf values of the object of the synthesis, 4,4′-dibromostilbene, and (dibenzofuran-2-yl)-phenylamine were respectively 0.37, 0.62, and 0.31, which were found by silica gel thin layer chromatography (TLC) (ethyl acetate:hexane (1:10) as the developing solvent).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08664263B2 |
| 出典データセット | uspto-grants-2014_03 |
| ORD ID | ord-fb94fe00aaea462a81b4c37cff3a3e99 |
| 出典メモ | uspto-grants-2014_03 |