化工社化工社 化学情報印刷レポート · 研究参考用
Diethylamine → H-Orn(Z)-OH
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylamine | HCID 8021 | — |
| 反応物 | Fmoc-orn(Z)-OH | HCID 14999635 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | H-Orn(Z)-OH | HCID 7009570 | 199.4% |
反応手順
The compound obtained in Example 8-5 (122.8 mg) was dissolved in DMF (2.6 ml). After the addition of diethylamine (0.26 ml), the mixture was stirred for 2 hours at room temperature. After the reaction, the solvent was removed by distillation under reduced pressure and the residue was dried under vacuum to obtain the title compound (133.5 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07098215B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-5fa1bf7313374de8b97081467abfed33 |
| 出典メモ | uspto-grants-2006_08 |