Tert-butyl 3-(benzylamino)benzoate → HCID 3681313、化合物
反応式
C([O:5][C:6](=[O:21])[C:7]1[CH:12]=[CH:11][CH:10]=[C:9]([NH:13][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH:8]=1)(C)(C)C>FC(F)(F)C(O)=O.ClCCl>[CH2:14]([NH:13][C:9]1[CH:8]=[C:7]([CH:12]=[CH:11][CH:10]=1)[C:6]([OH:21])=[O:5])[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1参加物
3
実験手順
A solution of 3-benzylamino-benzoic acid tert-butyl ester (1 g, 3 mmol) in trifluoroacetic acid/dichloromethane (1:5 v/v) (100 ml) was stirred for 16 hrs. The reaction was concentrated to dryness in vacuo to afford the title compound as a white solid. HPLC retention time 2.59 min. Mass spectrum (ES+) m/z 227.8 (M+).
後処理
- concentrationThe reaction was concentrated to dryness in vacuo
出典と根拠
- ORDレコード
- ord-7a40653fefc84916ba508f4b24ae9c11
- 出典データセット
- uspto-grants-2014_03
- 特許番号
- US08673901B2
反応ノート
読み込み中…