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Dichloromethane methanol → 8-(2-Chloro-5-methoxy-phenyl)-Quinoxaline-5-carboxylic acid (1H-imidazol-2-yl)amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dichloromethane methanol | HCID 21226129 | — |
| 反応物 | 8-(2-Chloro-5-methoxy-phenyl)-quinoxaline-5-carboxylic acid [3-(4-ethyl-piperazin-1-yl)-phenyl]-amide | HCID 44515980 | — |
| 生成物 | 8-(2-Chloro-5-methoxy-phenyl)-Quinoxaline-5-carboxylic acid (1H-imidazol-2-yl)amide | HCID 44516281 | — |
反応手順
The title compound was prepared in analogy to the procedures described in Example 14 but using 8-(2-chloro-5-methoxy-phenyl)-quinoxaline-5-carboxylic acid (Example 63) in Step 14.1. Title compound: ESI-MS: 380.0 [M+H]+; tR=3.61 min (System 1); TLC: Rf=0.36 (DCM/MeOH, 95:5).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08674099B2 |
| 出典データセット | uspto-grants-2014_03 |
| ORD ID | ord-61edd380963141d592eb901e67bbc2c5 |
| 出典メモ | uspto-grants-2014_03 |