化工社化工社 化学情報印刷レポート · 研究参考用
1-Amino-2-propanol → Tbpa mipa
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Amino-2-propanol | HCID 4 | — |
| 反応物 | Tributyl Phosphate | HCID 31357 | — |
| 生成物 | Tbpa mipa | HCID 131731251 | — |
反応手順
Reaction of TBPA with MIPA gives an TBPA/MIPA adduct. TBPA is sold in commerce by Albermarle as Saytex® RB-49. MIPA is sold in commerce by Dow Chemical. 44.8 mmol of TBPA is added to a round bottom flask with 50.74 grams of ethanol. The mixture is heated to reflux after which 44.8 mmol of MIPA is added dropwise and the solution refluxed for 1 hour. The ethanol is removed using a rotary evaporator to produce a yellow crystalline solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08679990B2 |
| 出典データセット | uspto-grants-2014_03 |
| ORD ID | ord-d6ca116be7344af0ad32793e54d9c541 |
| 出典メモ | uspto-grants-2014_03 |