化工社化工社 化学情報印刷レポート · 研究参考用
2-Bromoethanol → (4R,9aR)-6-(2-Hydroxy-ethoxy)-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromoethanol | HCID 10898 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | (4R,9aR)-6-bromo-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester | HCID 86590113 | — |
| 反応物 | HCID 178418747 | HCID 178418747 | — |
| 生成物 | (4R,9aR)-6-(2-Hydroxy-ethoxy)-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester | HCID 69556691 | — |
反応手順
This compound was prepared in analogy to Example 22 intermediate b), from (4R,9aR)-6-hydroxy-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester, sodium hydride and 2-bromoethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07098337B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-470b37aa1b554df0a01e828ed15e2e0e |
| 出典メモ | uspto-grants-2006_08 |