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Acrylic Acid → Ethylacrylate acrylic acid acrylonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Acrylonitrile | HCID 7855 | — |
| 反応物 | 1-Dodecanethiol | HCID 8195 | — |
| 反応物 | Ethyl Acrylate | HCID 8821 | — |
| 反応物 | Lauryl peroxide | HCID 76169 | — |
| 反応物 | Butyl perbenzoate | HCID 83282 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | Ethylacrylate acrylic acid acrylonitrile | HCID 168852 | — |
反応手順
this polymer material was produced by adding to 320g xylene at 100° C. the monomer solution and a catalyst solution over a period of 3 hours. The monomer solution contained 2.900g ethyl acrylate, 76g acrylonitrile, 76g acrylic acid and 3g laurylmercaptan. The catalyst solution contained 26g laurylperoxide and 7g butylperbenzoate in 273g of xylene. The material was highly viscous with comonomer proportions of 95:2.5:2.5.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04814215 |
| 出典データセット | uspto-grants-1989_03 |
| ORD ID | ord-b49eff8d34704bb290fcc0074a7ddde4 |
| 出典メモ | uspto-grants-1989_03 |