化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → p-Tolylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Lilac acetaldehyde | HCID 61006 | — |
| 反応物 | Sodium Hypochlorite | HCID 23665760 | — |
| 生成物 | p-Tolylacetic acid | HCID 248474 | — |
反応手順
In the like manner as Example 1, 26.4 g of p-methylphenylacetaldehyde as an aldehyde and 2.3 g of sulfuric acid were used. The oxidation was done by using 125 g of 12% aqueous solution of sodium hypochlorite at temperatures of -10° to -12° C., which was followed by the hydrogenation to obtain p-methylphenylacetic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04814494 |
| 出典データセット | uspto-grants-1989_03 |
| ORD ID | ord-a6c0e22ac83543e18b5dba56bc8d265d |
| 出典メモ | uspto-grants-1989_03 |