1-(4-Nitrophenyl)-N-(2-phenylethyl)methanesulfonamide → 1-(4-Aminophenyl)-N-(2-phenylethyl)methanesulfonamide

HRID 1194760ノート

反応式

HRID 1194760 の反応式
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][S:11]([NH:14][CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)(=[O:13])=[O:12])=[CH:6][CH:5]=1)([O-])=O>C(O)C>[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][S:11]([NH:14][CH2:15][CH2:16][C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)(=[O:13])=[O:12])=[CH:6][CH:5]=1

参加物

3

反応物 1

HCID 132861091-(4-Nitrophenyl)-N-(2-phenylethyl)methanesulfonamide

生成物 1

HCID 132861101-(4-Aminophenyl)-N-(2-phenylethyl)methanesulfonamide収率 94.6%

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒2 回

実験手順

By a procedure similar to that described in example 9(b) the product of stage (a) (7.0 g) was hydrogenated in ethanol to give the title compound as a white solid (6.0 g), m.p. 123°-125° (from ethanol).

出典と根拠

ORDレコード
ord-4295e888bdc64f9a8e4c462d328abe1b
出典データセット
uspto-grants-1989_03
特許番号
US04816470

反応ノート

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