HCID 19819017、化合物 → HCID 19819020、化合物

HRID 1195238ノート

反応式

HRID 1195238 の反応式
[ClH:1].[CH:2]1([C:5]([CH:7]2[CH2:9][CH2:8]2)=[NH:6])[CH2:4][CH2:3]1>CS(C)=O>[Cl-:1].[N+:6]12[CH2:9][CH2:8][CH2:7][C:5]=1[CH2:2][CH2:3][CH2:4]2

参加物

3

反応物 1

HCID 19819017HCID 19819017、化合物

生成物 1

HCID 19819020HCID 19819020、化合物収率 55%

試薬・触媒・溶媒 1

HCID 679Dimethyl Sulfoxide溶媒

反応条件

温度
100 °C

実験手順

A solution of dicyclopropylmethanimine hydrochloride (1.00 g, 6.87 mmol) in 6.0 ml of dimethyl sulfoxide was heated with stirring at 100° C. for 4 hours. The solvent was distilled out in vacuo and isobutyl alcohol (6 ml) was added to the residue. Precipitated crystals was obtained and dried in vacuo to afford 0.55 g (Yield: 55%) of the desired compound.

後処理

  1. distillationThe solvent was distilled out in vacuo and isobutyl alcohol (6 ml)
  2. additionwas added to the residue
  3. customPrecipitated crystals
  4. customwas obtained
  5. customdried in vacuo

出典と根拠

ORDレコード
ord-d0db1dab158242feb1f62fa127826663
出典データセット
uspto-grants-1992_05
特許番号
US05110945

反応ノート

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