Sodium 3-nitrobenzenesulfonate → 5-Hydroxy-8-methoxyquinoline

HRID 1195692

反応式

HRID 1195692 の反応式
[NH2:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[CH:6][C:7]=1[O:8][CH3:9].[N+]([C:14]1[CH:15]=C(S([O-])(=O)=O)C=C[CH:19]=1)([O-])=O.[Na+]>OCC(CO)O>[OH:10][C:4]1[CH:5]=[CH:6][C:7]([O:8][CH3:9])=[C:2]2[C:3]=1[CH:19]=[CH:14][CH:15]=[N:1]2

参加物

4

反応物 2

HCID 31389Sodium 3-nitrobenzenesulfonateHCID 203418413-Amino-4-methoxyphenol

生成物 1

HCID 1356893625-Hydroxy-8-methoxyquinoline

試薬・触媒・溶媒 1

HCID 753Glycerol溶媒

実験手順

Following the same procedure as in Example 23-(a), reaction and treatment were carried out using 2.25 g of 3-amino-4-methoxyphenol, 3.7 ml of glycerol and sodium m-nitrobenzene sulfonate to obtain 180 mg of 5-hydroxy-8-methoxyquinoline.

後処理

  1. customas in Example 23-(a), reaction and treatment

出典と根拠

ORDレコード
ord-be5a9f6acfc0441a8c45a7433e23392f
出典データセット
uspto-grants-1992_05
特許番号
US05112817

関連ノート

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