1-Pentanol → HCID 19896187、化合物

HRID 1196743

反応式

HRID 1196743 の反応式
O.[O:2]=[CH:3][C:4]([Cl:7])([Cl:6])[Cl:5].[CH2:8]([OH:13])[CH2:9][CH2:10][CH2:11][CH3:12]>C1C=CC=CC=1>[CH2:8]([O:2][CH:3]([O:13][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[C:4]([Cl:7])([Cl:6])[Cl:5])[CH2:9][CH2:10][CH2:11][CH3:12]

参加物

4

反応物 2

HCID 62761-PentanolHCID 205283762,2,2-Trichloroacetaldehyde hydrate

生成物 1

HCID 19896187HCID 19896187、化合物

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

A mixture of 5 g of chloral-hydrate, 10 ml of amyl-alcohol, 0.1 g of 4-methyl-sulphonic acid and 50 ml of benzene is kept at reflux temperature and the formed water is separated by means of a Dean-Stark apparatus. After a reaction time of 9 hours the benzene is washed with a sodium hydrogen carbonate solution and water, dried on magnesium sulfate, then it is vacuum-distilled.

後処理

  1. temperatureat reflux temperature
  2. customthe formed water is separated by means of a Dean-Stark apparatus
  3. washAfter a reaction time of 9 hours the benzene is washed with a sodium hydrogen carbonate solution and water
  4. customdried on magnesium sulfate
  5. distillationit is vacuum-distilled

出典と根拠

ORDレコード
ord-c1dab98a054a4eb980152bafb5a7767f
出典データセット
uspto-grants-1992_05
特許番号
US05116402

関連ノート

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