化工社化工社 化学情報印刷レポート · 研究参考用
Benzene → N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene | HCID 241 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | N-(4-methoxyphenyl)-3-methyl-4-nitrobenzamide | HCID 790964 | — |
| 生成物 | N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride | HCID 13633435 | — |
反応手順
14 g of N-(4-methoxyphenyl)-4-nitro-3-methyl benzamide in suspension in 70 ml of thionyl chloride were heated for 20 hours at reflux. The solvent was eliminated by entrainment with benzene, and after drying under reduced pressure at ambient temperature, 15 g of N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride melting towards 80° C. were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05278180 |
| 出典データセット | uspto-grants-1994_01 |
| ORD ID | ord-d6a32888520145e7b0f7ea42659d374a |
| 出典メモ | uspto-grants-1994_01 |