関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triethoxychlorosilane | HCID 78398 | — |
| 反応物 | Sodium acrylate | HCID 4068533 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Acryltriethoxysilane | HCID 21864273 | — |
反応手順
6.123 g (0.0651 mol) sodium acrylate is dissolved to 25 mL THF and cooled to −70° C. 12.8 mL (0.0651 mol, 12.938 g) chlorotriethoxysilane in THF (15 mL) is added dropwise to reaction solution. The solution is stirred for over night allowing it to warm up to room temperature. NaCl is removed by filtration and solution evaporated to dryness to result clear liquid, acryltriethoxysilane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07098346B2 |
|---|
| 出典データセット | uspto-grants-2006_08 |
|---|
| ORD ID | ord-ebe86df30b2441388fb356c07f9e4914 |
|---|
| 出典メモ | uspto-grants-2006_08 |
|---|
