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Propionitrile → HCID 178432489、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propionitrile | HCID 7854 | — |
| 反応物 | 1,2-Dimethylbenzimidazole | HCID 312693 | — |
| 反応物 | Disulfide, bis(2-bromoethyl) | HCID 572268 | — |
| 生成物 | HCID 178432489 | HCID 178432489 | — |
反応手順
2.4 g of 1,2-dimethylbenzimidazole, 2.1 g of bis(2-bromoethyl) disulfide and 6 ml of propionitrile were stirred at 100 C in a sealed 20 ml reactor for 8 h. After cooling, filtration, washing with 3 times 10 ml and drying under vacuum, 2.2 g of beige solid were recovered. The analyses showed that the product was in conformity with the expected structure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07727287B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-6ecb22d1266e4ad1878d98cb3b30a37b |
| 出典メモ | uspto-grants-2010_06 |