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alpha-Hydroxytriazolam → 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | alpha-Hydroxytriazolam | HCID 1963 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine acetate | HCID 70359440 | — |
反応手順
In a manner similar to Example 12, a mixture of 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine and acetic anhydride was heated on the water bath to give 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine acetate (ester).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04902794 |
| 出典データセット | uspto-grants-1990_02 |
| ORD ID | ord-56f90f3cd8f44867a19c25169971f8bd |
| 出典メモ | uspto-grants-1990_02 |