Hydrochloric Acid → HCID 14328079、化合物
反応式
[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:20]=[CH:19][C:14]3[NH:15][C:16](=[O:18])[O:17][C:13]=3[CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:21]>CO>[ClH:21].[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:20]=[CH:19][C:14]3[NH:15][C:16](=[O:18])[O:17][C:13]=3[CH:12]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1参加物
4
実験手順
A methanol solution (40 ml) containing 3.06 g of 6-(3-Phenylpropylamino)-2-benzoxazolone was combined with an ethereal solution saturated with gaseous hydrogen chloride (40 ml) at ice-bath temperature. The resulting solid was collected by filtration, washed with ether and dried to give the title compound (3.470 g).
後処理
- filtrationThe resulting solid was collected by filtration
- washwashed with ether
- customdried
出典と根拠
- ORDレコード
- ord-48b32ce60b624fd98ed44c4226548a80
- 出典データセット
- uspto-grants-1990_02
- 特許番号
- US04904685
反応ノート
読み込み中…