化工社化工社 化学情報印刷レポート · 研究参考用
Dicyclohexylcarbodiimide → Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | 2-Aminoxy-acetic acid ethyl ester | HCID 19808 | — |
| 反応物 | 4-Pentynoic acid | HCID 22464 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester | HCID 59336531 | — |
反応手順
To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07727713B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-128be03e30fc479198b6496eaff8785b |
| 出典メモ | uspto-grants-2010_06 |