関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2,3-Diaminotoluene | HCID 17593 | — |
| 反応物 | 6-Chloro-3-methoxypyridazine-4-carbaldehyde | HCID 84048811 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | HCID 178494311 | HCID 178494311 | — |
反応手順
6-Chloro-3-methoxypyridazine-4-carbaldehyde is dissolved in DMF, und 2,3-diaminotoluene is added. The reaction solution is heated at 120° C. in a microwave for 30 minutes. The crude product is purified on silica gel (eluent ethyl acetate in heptane). MS (ES+) m/z 275 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07727989B2 |
|---|
| 出典データセット | uspto-grants-2010_06 |
|---|
| ORD ID | ord-e986e39eba024f0d9b164fdcba6d54bc |
|---|
| 出典メモ | uspto-grants-2010_06 |
|---|
