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M-Cresol → t-butyl (1R)-2-(3-fluorophenoxy)-1-[(methylsulfanyl)methyl]ethylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | M-Cresol | HCID 342 | — |
| 反応物 | 3-Fluorophenol | HCID 9743 | — |
| 反応物 | t-butyl (1R)-2-hydroxy-1-[(methylsulfanyl)methyl]ethylcarbamate | HCID 15192846 | — |
| 生成物 | t-butyl (1R)-2-(3-fluorophenoxy)-1-[(methylsulfanyl)methyl]ethylcarbamate | HCID 86609357 | — |
反応手順
By the operation similar to that in Step 2 of Example 15 except that t-butyl (1R)-2-hydroxy-1-[(methylsulfanyl)methyl]ethylcarbamate (1 g) obtained in Step 1 was used as a starting material and m-cresol was changed to 3-fluorophenol, the title compound (300 mg) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728005B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-b06412e6adab493bad4027094337a0c0 |
| 出典メモ | uspto-grants-2010_06 |