化工社化工社 化学情報印刷レポート · 研究参考用
Carbon Disulfide → HCID 178507537、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbon Disulfide | HCID 6348 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | m-Aminobenzohydrazide | HCID 84178 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 178507537 | HCID 178507537 | — |
反応手順
3-Aminobenzhydrazide (5.76 g) was dissolved in ethanol (40 mL), and triethylamine (4.8 mL) and carbon disulfide (2.1 mL) were added to the solution. The mixture was heated under reflux for 4 hrs. The solvent was evaporated, and water was added. The precipitated solids were collected by filtration to give the title compound (5.06 g) as a pale-yellow powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07115635B2 |
| 出典データセット | uspto-grants-2006_10 |
| ORD ID | ord-2272d54bcda141169e47c2ffb68a7bea |
| 出典メモ | uspto-grants-2006_10 |