Methacrylic Acid → 2-Propenoic acid, 2-methyl-, trimethylsilyl ester
反応式
C(O[Si:5]([CH3:8])([CH3:7])[CH3:6])(=O)C.[C:9]([OH:14])(=[O:13])[C:10]([CH3:12])=[CH2:11]>CCCCCC>[C:9]([O:14][Si:5]([CH3:8])([CH3:7])[CH3:6])(=[O:13])[C:10]([CH3:12])=[CH2:11]参加物
4
実験手順
20 ml of acetoxytrimethylsilane and 11.4 ml of commercial methacrylic acid (ATOFINA Norsocryl® MAA) in 100 ml of hexane are mixed and heated. Azeotropic distillation of acetic acid affords trimethylsilyl methacrylate.
後処理
- temperatureheated
- distillationAzeotropic distillation of acetic acid
出典と根拠
- ORDレコード
- ord-84921c3b361f4ad9a245e308e86de751
- 出典データセット
- uspto-grants-2006_10
- 特許番号
- US07122692B2
反応ノート
読み込み中…