化工社化工社 化学情報印刷レポート · 研究参考用
2-Iodophenol → 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Iodophenol | HCID 10784 | — |
| 反応物 | Phenylboronic acid pinacol ester | HCID 570673 | — |
| 生成物 | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734623 | — |
反応手順
The above reaction procedure used for 2-iodophenol was followed. The reaction was faster, being complete before the first sample for gc analysis was withdrawn after 1 h 50 min reaction time. The amount of phenylboronic acid pinacol ester was higher than in the 2-iodophenol reaction (around 7%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07122694B2 |
| 出典データセット | uspto-grants-2006_10 |
| ORD ID | ord-23004de992854d06895bd83361499298 |
| 出典メモ | uspto-grants-2006_10 |