化工社化工社 化学情報印刷レポート · 研究参考用
13-cis-Acitretin → Acitretin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 13-cis-Acitretin | HCID 6437841 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | Acitretin | HCID 5284513 | 98.3% |
反応手順
Crude acetretin (10 g) was added to acetone (300 ml) and stirred at 25–30° C. for 1 hour under nitrogen atmosphere. The suspension was then filtered, washed with acetone (100 ml) and dried under vacuum at 25–30° C. to obtain pure acitretin (8 g, Assay 98.3% by HPLC).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07129365B2 |
| 出典データセット | uspto-grants-2006_10 |
| ORD ID | ord-0a6a1dd62a144e049522c3ad6075d89a |
| 出典メモ | uspto-grants-2006_10 |