3-Ethoxy-1-(3-pyridinyl)-2-propen-1-one → HCID 13475883、化合物

HRID 1247953

反応式

HRID 1247953 の反応式
C(O[CH:4]=[CH:5][C:6]([C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)=O)C.[NH2:14][C:15]1[C:19]([C:20]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[O:21])=[CH:18][NH:17][N:16]=1>C1(C)C(C)=CC=CC=1>[C:22]1([C:20]([C:19]2[CH:18]=[N:17][N:16]3[C:6]([C:8]4[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=4)=[CH:5][CH:4]=[N:14][C:15]=23)=[O:21])[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1

参加物

4

反応物 2

HCID 540323263-Ethoxy-1-(3-pyridinyl)-2-propen-1-oneHCID 178509267HCID 178509267、化合物

生成物 1

HCID 13475883HCID 13475883、化合物

試薬・触媒・溶媒 1

HCID 7237O-Xylene溶媒

実験手順

A mixture of 0.02 mole of 3-ethoxy-1-(3-pyridinyl)-2-propen-1-one, 0.02 mole of (3-amino-1H-pyrazol-4-yl)phenyl-methanone and 100 ml of xylene was refluxed for 12 hours. The solvent was removed and the residue dissolved in dichloromethane. This solution was dried over sodium sulfate and the product isolated as described in Example 1, as crystals, mp 202°-203° C.

後処理

  1. temperaturewas refluxed for 12 hours
  2. customThe solvent was removed
  3. dissolutionthe residue dissolved in dichloromethane
  4. dry with materialThis solution was dried over sodium sulfate
  5. customthe product isolated

出典と根拠

ORDレコード
ord-c49638eb094243959a97d943725eda29
出典データセット
uspto-grants-1985_06
特許番号
US04521422

関連ノート

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