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Dimethylamine → HCID 12797674、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Quizalofop | HCID 178795 | — |
| 生成物 | HCID 12797674 | HCID 12797674 | 91% |
反応手順
In 30 ml. of 10% aqueous solution of dimethylamine, 3.4 g. (0.01 mole) of 2-[4-(6-chloro-2-quinoxalyloxy)phenoxy]propionic acid was added. After a dissolution, excess of dimethylamine and water were removed by evaporating them by a rotary evaporator and the residue was dried in vacuum to obtain 3.5 g. (yield: 91%) of a pale yellow object product having a melting point of 63° to 67° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04629493 |
| 出典データセット | uspto-grants-1986_12 |
| ORD ID | ord-a32bfccf63e94fdaaa45716d226bb358 |
| 出典メモ | uspto-grants-1986_12 |