Diethylamine → HCID 13090789、化合物
反応式
[Cl:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[C:7]([Cl:12])[C:6]=2[CH2:13]Cl.[CH2:15]([NH:17][CH2:18][CH3:19])[CH3:16]>O>[Cl:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[C:7]([Cl:12])[C:6]=2[CH2:13][N:17]([CH2:18][CH3:19])[CH2:15][CH3:16]参加物
4
実験手順
24.6 parts of 3,7-dichloro-8-chloromethylquinoline and 30 parts of diethylamine were stirred at 55° C. for 6 hours. Water was added and the solid was filtered off with suction and dried. 25 parts of 3,7-dichloro-8-diethylaminomethylquinoline of melting point 54° C. were obtained. The yield corresponds to 89% of theory.
後処理
- filtrationthe solid was filtered off with suction
- customdried
出典と根拠
- ORDレコード
- ord-51ef6f01f8d4406891977dbb2b8a36fb
- 出典データセット
- uspto-grants-1986_12
- 特許番号
- US04632696
反応ノート
読み込み中…