Hydrochloric Acid → Leucocrystal Violet

HRID 1249603

反応式

HRID 1249603 の反応式
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH3:12][N:13]([CH3:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.Cl>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]([C:6]2[CH:9]=[CH:10][C:3]([N:2]([CH3:11])[CH3:1])=[CH:4][CH:5]=2)[C:17]2[CH:18]=[CH:19][C:14]([N:13]([CH3:20])[CH3:12])=[CH:15][CH:16]=2)=[CH:5][CH:4]=1

参加物

4

反応物 3

HCID 313Hydrochloric AcidHCID 949N,N-DimethylanilineHCID 74794-(Dimethylamino)Benzaldehyde

生成物 1

HCID 69048Leucocrystal Violet収率 189.9%

反応条件

温度
100 °C

実験手順

A mixture consisting of 44.76 g (0.3 mole) of the 4-dimethylaminobenzaldehyde thus obtained, 76.3 g (0.63 mole) of dimethylaniline and 247 g of a 20% aqueous HCl solution was condensed by stirring it at 100° C. for 8 hours to obtain 106.4 g of tris(4-dimethylaminophenyl)methane.

後処理

  1. customthus obtained
  2. customcondensed

出典と根拠

ORDレコード
ord-d9c1a2cec0f940ffb64e4be0c91b7a5c
出典データセット
uspto-grants-1986_12
特許番号
US04632987

関連ノート

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