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N-Vinylpyrrolidine → Ethyl 5-phenyl-6-(4-trifluoromethylphenyl)-pyridine-2-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Vinylpyrrolidine | HCID 3014294 | — |
| 反応物 | Ethyl 5-(4-trifluoromethylphenyl)-6-phenyl-1,2,4-triazine-3-carboxylate | HCID 59338807 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Ethyl 5-phenyl-6-(4-trifluoromethylphenyl)-pyridine-2-carboxylate | HCID 68407826 | — |
反応手順
Following General Procedure D, ethyl 5-(4-trifluoromethylphenyl)-6-phenyl-1,2,4-triazine-3-carboxylate (Compound 19, 1 g, 2.68 mmol) and crude 1-vinylpyrrolidine (Compound 38, 1.4 g) in CHCl3 (20 ml) were reacted to produce the title compound as a yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728014B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-44b6bfd75d794d3281b750bfa16d6f38 |
| 出典メモ | uspto-grants-2010_06 |