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Ethyl 6-Phenyl-5-(4-trifluoromethylphenyl)-pyridine-2-carboxylate → Methyl 6-Phenyl-5-(4-trifluoromethylphenyl)-pyridine-2-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 6-Phenyl-5-(4-trifluoromethylphenyl)-pyridine-2-carboxylate | HCID 68408073 | — |
| 触媒 | Sulfuric Acid | HCID 1118 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Methyl 6-Phenyl-5-(4-trifluoromethylphenyl)-pyridine-2-carboxylate | HCID 25033166 | — |
反応手順
Following General Procedure E, ethyl 6-phenyl-5-(4-trifluoromethylphenyl)-pyridine-2-carboxylate (Compound 25, 110 mg, 0.29 mmol) and conc. H2SO4 (5 drops) in MeOH (5 ml) were reacted to produce the title compound as a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728014B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-c1134c48fb9443239d86e6435989bfb3 |
| 出典メモ | uspto-grants-2010_06 |