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HRID 1253165作成日：2026年10月27日

Ammonium Chloride → 5-(4-[2-Propylguanidino]pyrimid-2-yl)valeramidine hydrochloride

https://huagongshe.com/reaction/1253165

反応式

関与物質

役割名称HCID仕込み量
反応物Ammonium ChlorideHCID 25517—
反応物Methyl 5-(4-[2-propylguanidino]pyrimid-2-yl)valerimidateHCID 20137162—
溶媒MethanolHCID 887—
生成物5-(4-[2-Propylguanidino]pyrimid-2-yl)valeramidine hydrochlorideHCID 2013714993.2%

反応手順

A mixture of methyl 5-(4-[2-propylguanidino]pyrimid-2-yl)valerimidate (0.4 g.) and ammonium chloride (0.076 g.) in MeOH (20 ml.) was stirred at ambient temperature for 1 hour and the solvent evaporated in vacuo to give 5-(4-[2-propylguanidino]pyrimid-2-yl)valeramidine hydrochloride (0.4 g.) as an oil which was used without further purification.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04748165
出典データセットuspto-grants-1988_05
ORD IDord-9f68561694d34a0d9c0e9e77265079fc
出典メモuspto-grants-1988_05