Ammonia → HCID 20137143、化合物
反応式
[CH3:1][NH:2][C:3](=S)[NH:4][C:5]1[CH:9]=[N:8][N:7]([CH2:10][CH2:11][CH2:12][CH2:13][C:14]#[N:15])[N:6]=1.[NH3:17]>>[CH3:1][N:2]=[C:3]([NH2:17])[NH:4][C:5]1[CH:9]=[N:8][N:7]([CH2:10][CH2:11][CH2:12][CH2:13][C:14]#[N:15])[N:6]=1参加物
3
実験手順
A solution of 5-[4-(3-methylthioureido)1,2,3-triazol-2-yl]valeronitrile in methanolic ammonia (6M; 15 ml.) was treated with mercuric oxide (1.1 g.) and tne mLxture stirred for 3 hours at room temperature. The resulting suspension was filtered through diatomaceous earth and the filtrate evaporated to give 5-[4-(2-methylguanidino)-1,2,3-triazol-2-yl]valeronitrile as a yellow oil.
後処理
- filtrationThe resulting suspension was filtered through diatomaceous earth
- customthe filtrate evaporated
出典と根拠
- ORDレコード
- ord-52280a94928b44df9c533c8d4d2d65e5
- 出典データセット
- uspto-grants-1988_05
- 特許番号
- US04748165
反応ノート
読み込み中…