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4-Pyridinecarboxaldehyde → Ethyl 3-(4-Ethylphenyl)-[2,4']-bipyridinyl-6-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| 反応物 | 3-Ethoxycarbonyl-1,1,1-triphenyl-6-(4-ethylphenyl)-2-aza-1lambda5-phosphahexa-1,3,5-triene | HCID 86619069 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | Ethyl 3-(4-Ethylphenyl)-[2,4']-bipyridinyl-6-carboxylate | HCID 68408497 | — |
反応手順
Following General Procedure K, 4-pyridinecarboxaldehyde (92 mg, 0.86 mmol) and 3-ethoxycarbonyl-1,1,1-triphenyl-6-(4-ethylphenyl)-2-aza-1λ5-phosphahexa-1,3,5-triene (Compound 46, 434 mg, 0.86 mmol) in dry acetonitrile (10 ml) were reacted to produce the title compound as a yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728014B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-785262fa1aa54b4eaa636014f7b15a5e |
| 出典メモ | uspto-grants-2010_06 |