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Picolinate → Methyl 5-(4-ethylphenyl)-6-(pyridin-2-yl)pyridine-2-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Picolinate | HCID 6920223 | — |
| 反応物 | Ethyl 3-(4-Ethylphenyl)-[2,2']-bipyridinyl-6-carboxylate | HCID 68409104 | — |
| 触媒 | Sulfuric Acid | HCID 1118 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Methyl 5-(4-ethylphenyl)-6-(pyridin-2-yl)pyridine-2-carboxylate | HCID 59338839 | — |
反応手順
Following General Procedure E, ethyl 5-(4-ethylphenyl)-6-(pyridine-2-yl)phenyl)pyridine-2-carboxylate (Compound 50, 16 mg, 0.05 mmol) and conc. H2SO4 (10 drops) in methanol were reacted to produce the title compound as a light yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728014B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-f84eb07691ad48848f4d45b22cacaa43 |
| 出典メモ | uspto-grants-2010_06 |