化工社化工社 化学情報印刷レポート · 研究参考用
Diethyl Oxalate → 3,4-Dihydroxy-thiophene-2,5-dicarboxylic acid diethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethyl Oxalate | HCID 7268 | — |
| 反応物 | Diethyl 2,2'-thiodiacetate | HCID 70216 | — |
| 生成物 | 3,4-Dihydroxy-thiophene-2,5-dicarboxylic acid diethyl ester | HCID 245503 | — |
反応手順
The diethyl thioglycolate and diethyl oxalate are mixed, and then added to a first solution containing a first electron donor in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 100-500 W to perform a condensation reaction for 20-60 minutes to obtain 2,5-diethoxycarbonyl-3,4-dihydroxythiophene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08461355B2 |
| 出典データセット | uspto-grants-2013_06 |
| ORD ID | ord-143650d936db48c582b83b33620e8e81 |
| 出典メモ | uspto-grants-2013_06 |