化工社化工社 化学情報印刷レポート · 研究参考用
Nitric Acid → Magnesium nitrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Aluminum nitrate nonahydrate | HCID 24567 | — |
| 反応物 | Magnesium nitrate | HCID 25212 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Magnesium nitrate | HCID 25212 | — |
| 生成物 | Aluminum nitrate | HCID 26053 | — |
反応手順
An aqueous solution in which 3.75 kg of aluminum nitrate nonahydrate, 2.56 kg of magnesium nitrate and 540 g of 60% nitric acid were dissolved in 5.0 L of pure water was gradually dropped into 20.0 kg of a stirred silica sol solution having a colloidal particle diameter of from 10 to 20 nm held at 15° C. (Snowtex N-30 manufactured by Nissan Chemical Industries, Ltd. (SiO2 content: 30% by mass)) to obtain a mixed slurry of silica sol, aluminum nitrate and magnesium nitrate. Subsequently, the mixed slurry was aged by holding at 50° C. for 24 hours. After cooling to room temperature, the mixed slurry was spray-dried with a spray dryer set to an outlet temperature of 130° C. to obtain a solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08461373B2 |
| 出典データセット | uspto-grants-2013_06 |
| ORD ID | ord-b4a316090f7643fd8f1e7dfcf0228e5e |
| 出典メモ | uspto-grants-2013_06 |