Triethylamine → 2,4,6-Triiodophenyl penta-4-enoate
反応式
[CH:1]1[C:2]([I:10])=[CH:3][C:4]([I:9])=[C:5]([OH:8])[C:6]=1[I:7].[C:11](Cl)(=[O:16])[CH:12]=[CH:13][CH2:14][CH3:15].C(N(CC)CC)C>ClCCl>[C:11]([O:8][C:5]1[C:6]([I:7])=[CH:1][C:2]([I:10])=[CH:3][C:4]=1[I:9])(=[O:16])[CH2:12][CH2:13][CH:14]=[CH2:15]参加物
5
実験手順
First, 9 g of triiodophenol was dissolved in 150 mL dichloromethane under argon. Then, 3.15 mL of pentenoyl chloride was added while stirring. Triethylamine was then added slowly and stirred for 4 hr. The solution was washed with 100 mL of water and evaporated to dryness, leaving 2,4,6-triiodophenyl penta-4-enoate.
後処理
- stirringstirred for 4 hr
- washThe solution was washed with 100 mL of water
- customevaporated to dryness
出典と根拠
- ORDレコード
- ord-f5ec7c7b42c14d5aadebb227c5c52ac9
- 出典データセット
- uspto-grants-2013_06
- 特許番号
- US08470035B2
反応ノート
読み込み中…