2,6-Di-tert-butyl-4-mercaptophenol → HCID 13547658、化合物
反応式
[C:1]([C:5]1[CH:10]=[C:9]([SH:11])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]=1[OH:16])([CH3:4])([CH3:3])[CH3:2].[CH2:17]([N:21]1[C:25](=[O:26])[CH:24]=[CH:23][C:22]1=[O:27])[CH2:18][CH2:19][CH3:20]>C(N(CC)CC)C>[CH2:17]([N:21]1[C:25](=[O:26])[CH2:24][CH:23]([S:11][C:9]2[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]([OH:16])=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:10]=2)[C:22]1=[O:27])[CH2:18][CH2:19][CH3:20]参加物
4
実験手順
The procedure of Example 1 is repeated using 11.92 grams 2,6-di-tert-butyl-4-mercaptophenol, 7.66 grams N-n-butylmaleimide, and 0.5 grams triethylamine. The residue is purified by dry column chromatography to give a white solid, m.p. 80°-85° C.
後処理
- customThe residue is purified
- customby dry column chromatography