化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → Methyl 4-formamidothiophene-3-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Methyl 4-aminothiophene-3-carboxylate | HCID 2777610 | — |
| 反応物 | Sodium Acetate Trihydrate | HCID 23665404 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Methyl 4-formamidothiophene-3-carboxylate | HCID 2777637 | — |
反応手順
A stirred solution of methyl 4-amino-3-thenoate (4 g), sodium acetate trihydrate (2.8 g) and formic acid (27 ml) was heated at 95° C. for 1 hour. On cooling the solution was poured into water, and the solution filtered to give the title product as a solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06541630B1 |
| 出典データセット | uspto-grants-2003_04 |
| ORD ID | ord-1f8a736f815c4486ba73f995478a54f7 |
| 出典メモ | uspto-grants-2003_04 |