反応式
[N+:1]([C:4]1[C:5](S([O-])(=O)=O)=[N:6][CH:7]=[CH:8][C:9]=1[NH2:10])([O-:3])=[O:2].[CH2:15]([NH:22][CH2:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[CH2:23]([N:22]([CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:5]1[C:4]([N+:1]([O-:3])=[O:2])=[C:9]([NH2:10])[CH:8]=[CH:7][N:6]=1)[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1参加物
3
実験手順
In step (2) of Reaction Scheme I a 3-nitro-4-aminopyridine-2-sulfonate of Formula XI is reacted with dibenzylamine to provide a 2-dibenzylamino-3-nitropyridin-4-amine of Formula XII. The reaction is carried out by combining a compound of Formula XI, dibenzylamine, and a tertiary amine such as triethylamine in an inert solvent such as benzene, toluene or xylene and heating the resulting mixture.
出典と根拠
- ORDレコード
- ord-0bdcefb2a0cb4fec8c1c8d47a19d09f1
- 出典データセット
- uspto-grants-2003_04
- 特許番号
- US06545017B1
関連ノート
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