Perfluorooctanesulfonic acid → HCID 22726281、化合物

HRID 1265963

反応式

HRID 1265963 の反応式
[F:1][C:2]([F:29])([S:25]([OH:28])(=[O:27])=[O:26])[C:3]([F:24])([F:23])[C:4]([F:22])([F:21])[C:5]([F:20])([F:19])[C:6]([F:18])([F:17])[C:7]([F:16])([F:15])[C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[F:10].C(=O)([O-])[O-].[Ag+2:34]>O>[F:29][C:2]([F:1])([S:25]([O-:28])(=[O:27])=[O:26])[C:3]([F:23])([F:24])[C:4]([F:22])([F:21])[C:5]([F:19])([F:20])[C:6]([F:18])([F:17])[C:7]([F:16])([F:15])[C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[F:10].[Ag+:34]

参加物

4

反応物 2

HCID 74483Perfluorooctanesulfonic acidHCID 178418647HCID 178418647、化合物

生成物 1

HCID 22726281HCID 22726281、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

後処理

  1. additionwas added
  2. stirringAfter stirring at room temperature for 3 days
  3. filtrationthe mixture was filtered
  4. filtrationthe obtained filter-cake
  5. washwas washed with 10 parts of ion-exchange water
  6. dry with material20 parts of diethylether and dried

出典と根拠

ORDレコード
ord-6ac8754eaec44102a8cb06ad7b0bca55
出典データセット
uspto-grants-2003_04
特許番号
US06548221B2

関連ノート

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