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2-Methoxyethanol → 5-(2-Methoxy-ethoxy)-2-nitro-4-pyrrol-1-yl-phenylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methoxyethanol | HCID 8019 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | 5-(2-Methoxy-ethoxy)-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548743 | — |
反応手順
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (1.01 g, 4 mmol), 2-methoxyethanol (1.58 mL, 20 mmol) and KOH (316 mg, 4.8 mmol) in DMSO (5 mL) according to the general procedure E. Obtained as an orange solid (870 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06548495B2 |
| 出典データセット | uspto-grants-2003_04 |
| ORD ID | ord-9e9db5af966b4cfca83cab6f3020956a |
| 出典メモ | uspto-grants-2003_04 |