化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548717 | — |
反応手順
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (5.94 g, 25 mmol), methanol (25 mL) and KOH (1.98 g, 30 mmol) in DMSO (25 mL) according to the general procedure E. Obtained as an orange solid (5.88 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06548495B2 |
| 出典データセット | uspto-grants-2003_04 |
| ORD ID | ord-e6ee15db5ebc44d9980b62679a2b0bb5 |
| 出典メモ | uspto-grants-2003_04 |