化工社化工社 化学情報印刷レポート · 研究参考用
Methylamine → HCID 20571388、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylamine | HCID 6329 | — |
| 反応物 | Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)- | HCID 16197 | — |
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 生成物 | HCID 20571388 | HCID 20571388 | — |
反応手順
Following the methods of Example 1, 2-(4-chlorophenyl)-3-methylbutanoic acid is reacted with oxalyl chloride and aqueous methylamine to give N-methyl-2-(4-chlorophenyl)-3-methylbutyramide, which is then combined with 3-phenoxybenzyl bromide and AgBF4, yielding 3-phenoxybenzyl N-methyl-2-(4-chlorophenyl)-3-methylbutanimidate, MS m/e 407 (M+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04254264 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-f22e67409f3745d498d28c7d45897e05 |
| 出典メモ | uspto-grants-1981_03 |